In-situ tensile testing of propellants in SEM

In-situ tensile testing of propellants in SEM: Influence of temperature

di Benedetto, G.L.
van Ramshorst, M.C.J.
Duvalois, W.
Hooijmeijer, P.A.
van der Heijden, A.E.D.M.

2017

A tensile module system placed within a Scanning Electron Microscope (SEM) was utilized to conduct insitu tensile testing of propellant samples. The tensile module system allows for real-time in-situ SEM analysis of the samples to determine the failure mechanism of the propellant material under tensile force. The focus of this study was to vary the experimental parameters of the tensile module system and analyze how they affect the failure mechanism of the samples. The experimental parameters varied included strain rate and sample temperature ( 54, +25 and +408C). Stress-strain diagrams were recorded during the in-situ tensile tests, and these results were coupled with the in-situ images and videos of the samples captured with SEM analysis. The experiments conducted at 548C showed a different failure behavior of the propellant sample due to its rigidity at this low temperature, while experiments conducted at +25 and +408C displayed a similar failure mechanism. For future testing using this tensile tester, special attention should be given to improved temperature control of the specimen, especially at low temperatures.

Propellants
Micromechanical deformation
In-situ tensile testing
In-situ SEM
Scanning Electron Microscopy
Temperature effect
Defence Research
Defence, Safety and Security
Observation, Weapon & Protection Systems
EM - Energetic Materials
TS - Technical Sciences

http://resolver.tudelft.nl/uuid:24aea94b-0511-4355-a984-9655abbf4246

https://doi.org/10.1002/prep.201700178

782579

Wiley, Weinheim

Propellants Explosives Pyrotechnics, 42 (42), 1396-1400

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